DIY Herbal Shampoo Bars (All Hair Types): Gentle Recipes + Custom Herbal Add-Ins

You can make effective, gentle shampoo bars at home without harsh chemicals or confusing chemistry. This guide covers two beginner-friendly recipes—a syndet (no-lye) bar that works for most hair types, and a sensitive scalp option—plus a customization system so you can dial in herbs, clays, and add-ins for your exact hair needs. You'll learn the difference between syndet bars and traditional soap bars, how to avoid waxy residue, and exactly what to do if things go wrong.

Finished shampoo bars on a wooden tray with fresh herbs Alt text: "Handmade herbal shampoo bars with rosemary and nettle on rustic wood surface"
Finished shampoo bars


Why "All Hair Types" Needs Customization (Not Magic)

Here's the truth: no single shampoo bar works perfectly for everyone straight out of the gate. Your hair type, water hardness, and scalp needs all matter.

But here's the good news: you can build a shampoo bar that works for YOU by starting with a gentle base formula and adding targeted herbs, clays, or conditioning agents based on what your hair actually needs.

Think of it like cooking. The base recipe is your foundation. The add-ins are your flavor adjustments.

This guide gives you both: solid base recipes that won't strip or build up on most hair types, plus a customization framework so you're not guessing which herbs to throw in.

Shampoo Bar vs Hair Soap (Why pH Matters)

Let's clear up the confusion right now.

Shampoo bars and hair soaps are not the same thing.

Soap-Based Bars (Traditional Cold Process)

  • Made with oils + lye (sodium hydroxide)
  • The lye converts oils into soap through saponification
  • Typically have a pH of 8–10 (alkaline)
  • Hair's natural pH is around 4.5–5.5 (slightly acidic)
  • The mismatch: Alkaline soap opens the hair cuticle, which can feel rough, tangled, or leave residue—especially in hard water
  • Who it works for: Some people love them (especially with soft water and an acidic rinse), but they require technique and adjustment

Syndet Shampoo Bars (Synthetic Detergent Bars)

  • Made with gentle surfactants (like SCI or SCS)—no lye involved
  • Can be formulated to a pH closer to hair's natural range (~5–6)
  • Less likely to cause waxy buildup or that "stripped then greasy rebound" cycle
  • Who it works for: Most hair types, especially beginners, hard water areas, or anyone who's had bad experiences with soap bars

Which should you make?

If you're new to DIY shampoo bars or have had waxy/tangled results before, start with a syndet bar. They're more forgiving.

If you love the idea of a fully from-scratch soap bar and have soft water (or don't mind vinegar rinses), soap-based bars can be beautiful—but they're not for everyone.

This guide focuses on syndet recipes because they deliver the "all hair types" promise more reliably.

Choose Your Method: Decision Framework

START HERE | v Do you have access to SCI (Sodium Cocoyl Isethionate)? | +---> YES --> Make Recipe #1: Gentle Herbal Syndet Bar | (Beginner-friendly, works for most hair types) | +---> NO, but I can order online --> Order SCI + make Recipe #1 | +---> NO, and I want to use what I have --> Consider soap-based (not covered in detail here; requires lye safety knowledge) Do you have sensitive skin/scalp or fragrance sensitivity? | +---> YES --> Make Recipe #2: Sensitive Scalp Bar (Low scent, no essential oils option, gentle surfactants)

Decision Flowchart - Before decision box (visual guide)
Decision Flowchart


Tools + Ingredients You'll Need

Ingredients flatlay: All ingredients measured in bowls with labels Alt text: "DIY shampoo bar ingredients including SCI powder, BTMS, oils, and dried herbs arranged on white background"
Ingredients


Essential Tools

  • Digital scale (accurate to 1g)
  • Heat-safe bowl or double boiler
  • Silicone spatula
  • Silicone molds (soap molds, muffin tins, or small silicone ice cube trays work)
  • Optional: immersion blender for faster mixing

Shopping Checklist (Base Ingredients)

For Syndet Bars:

  • SCI (Sodium Cocoyl Isethionate) powder or noodles
  • BTMS-25 or BTMS-50 (conditioning emulsifier)
  • Cocamidopropyl betaine (optional, adds lather)
  • Carrier oil (like jojoba, argan, or sweet almond)
  • Panthenol (pro-vitamin B5, optional but recommended)
  • Distilled water or herbal infusion
  • Preservative (Leucidal SF or Optiphen Plus if adding water-based ingredients)

Herbal Add-Ins (choose 1–3):

  • Dried rosemary (stimulating, for all hair types)
  • Nettle leaf (strengthening, mineral-rich)
  • Chamomile (soothing, brightening for light hair)
  • Hibiscus (shine, color deposit for dark/red tones)
  • Amla powder (conditioning, prevents premature graying)
  • Calendula (calming for sensitive scalps)

Texture/Function Add-Ins:

  • Kaolin or bentonite clay (oil control, 1–2 tsp per batch)
  • Hydrolyzed wheat protein (strength, 1–2 tsp)
  • Essential oils (optional: rosemary, lavender, peppermint—use at 1–2%)

Recipe #1: Gentle Herbal Syndet Shampoo Bar (All Hair Types)

Gentle Herbal Syndet Shampoo Bar

Yield: 4–6 bars (depending on mold size) Difficulty: Beginner Prep time: 15 minutes Set time: 24–48 hours

Ingredients (by weight)

Ingredient

Grams

Ounces (approx)

Purpose

SCI powder

100g

3.5 oz

Gentle cleansing surfactant

BTMS-25

20g

0.7 oz

Conditioning, detangling

Cocamidopropyl betaine

10g

0.35 oz

Lather boost (optional)

Jojoba oil

10g

0.35 oz

Scalp nourishment

Panthenol

5g

0.17 oz

Slip, moisture retention

Rosemary + nettle infusion*

15g

0.5 oz

Herbal benefits

Kaolin clay

5g

0.17 oz

Oil control (omit for dry hair)

Preservative (Leucidal SF)

3g

0.1 oz

Prevents mold if using water

Essential oil blend (optional)

2g

0.07 oz

Scent


Total batch weight: ~170g

*To make herbal infusion: Steep 1 tbsp each dried rosemary + nettle in 1/4 cup boiling distilled water for 30 min. Strain completely.

"Melting sodium cocoyl isethionate in glass bowl over double boiler for shampoo bar recipe"
Melting SCI in double boiler

Instructions

  1. Prep your herbs: Make the infusion and let it cool. Strain well—no plant bits should remain.
  2. Melt the base: In a heat-safe bowl over a double boiler, combine SCI powder and BTMS-25. Heat gently, stirring occasionally, until melted and combined (this can take 10–15 minutes; SCI is stubborn).
  3. Add liquids: Remove from heat. Stir in jojoba oil, panthenol, and cocamidopropyl betaine. Mix thoroughly.
  4. Add herbal infusion: Slowly add your cooled infusion while stirring. The mixture will thicken quickly.
  5. Add clay + preservative: Sprinkle in kaolin clay and preservative. Mix until evenly distributed.
  6. Add essential oils (if using): Stir in your essential oil blend.
  7. Mold immediately: The mixture will be thick and putty-like. Press firmly into molds, packing tightly to avoid air pockets.
  8. Set: Let bars sit in molds for 24 hours at room temperature. Pop out and let cure on a rack for another 24–48 hours before use.
Hand mixing thick shampoo bar mixture with spatula showing putty-like texture
Mixing thick shampoo bar paste


Substitutions

  • No SCI? Try SCS (Sodium Coco Sulfate) at the same ratio—slightly different feel, still works.
  • No BTMS? Use cetyl alcohol (15g) + polysorbate 80 (5g)
  • No jojoba? Swap for argan, sweet almond, or light olive oil
  • No herbal infusion? Use plain distilled water or skip liquid entirely (bar will be harder to mol,d but still works)

Recipe #2: Simple Sensitive Scalp Herbal Bar (Low Scent / No Essential Oils Option)

Simple Sensitive Scalp Herbal Bar

Yield: 4–6 bars Difficulty: Beginner. Best for: Sensitive skin, eczema-prone scalps, fragrance sensitivity

Ingredients (by weight)

Ingredient

Grams

Ounces (approx)

Purpose

SCI powder

110g

3.9 oz

Extra-gentle cleansing

BTMS-50

25g

0.9 oz

Higher conditioning for soothing

Sweet almond oil

15g

0.5 oz

Calming, non-irritating

Calendula infusion*

10g

0.35 oz

Anti-inflammatory

Colloidal oatmeal

5g

0.17 oz

Scalp soothing

Panthenol

5g

0.17 oz

Moisture without weight

Preservative (Leucidal SF)

3g

0.1 oz

Safety


Total batch weight: ~173g

*Calendula infusion: Steep 1 tbsp dried calendula in 1/4 cup boiling distilled water for 30 min. Strain.

Instructions

Follow the same method as Recipe #1:

  1. Melt SCI + BTMS-50
  2. Add sweet almond oil + panthenol
  3. Stir in calendula infusion slowly
  4. Add colloidal oatmeal + preservative
  5. Skip essential oils (or use chamomile at 0.5% if tolerated)
  6. Mold, set 24 hours, cure 24–48 hours

Customize by Hair Type

Start with either base recipe, then dial in these add-ins:

For Oily Hair / Scalp

  • Add: 1 tsp bentonite clay or rhassoul clay
  • Add: Nettle or rosemary infusion (both help balance oil)
  • Reduce: Oils slightly (use 8g instead of 10–15g)
  • Essential oils: Peppermint, tea tree (1% total)

For Dry, Curly, or Coarse Hair

  • Add: 5–10g extra conditioning oil (argan, avocado, or shea butter)
  • Add: Hibiscus or amla infusion (shine + slip)
  • Add: 1 tsp hydrolyzed wheat protein (strengthens without drying)
  • Skip: Clay
  • Essential oils: Lavender, ylang ylang (1–2%)

For Fine or Thin Hair

  • Keep oils light: Jojoba or grapeseed (avoid heavy butters)
  • Add: Rosemary infusion (stimulates scalp)
  • Add: Panthenol for volume without weight
  • Optional: 1/2 tsp kaolin clay for gentle oil control
  • Essential oils: Rosemary, cedarwood (1%)

For Color-Treated or Damaged Hair

  • Add: 1 tsp hydrolyzed wheat or silk protein
  • Add: Chamomile (brightens) or hibiscus (color deposit for reds/browns)
  • Increase: BTMS to 25–30g for extra conditioning
  • Essential oils: Geranium, lavender (1%)

For Dandruff-Prone or Itchy Scalp

  • Add: Nettle + calendula infusion
  • Add: 1 tsp neem powder (antifungal, strong scent—use sparingly)
  • Essential oils: Tea tree + rosemary (1.5% total)
  • Note: If dandruff persists, consult a dermatologist—it may need medical treatment

How to Use Your Shampoo Bar

First-time users: Your hair may need 2–4 washes to adjust, especially if switching from conventional shampoo.

Wash-Day Technique Checklist

  • Wet hair thoroughly with warm water (really soak it)
  • Wet the bar and rub between hands to create lather, OR
  • Rub bar directly on scalp in gentle circular motions (roots only)
  • Massage scalp with fingertips for 1–2 minutes—let the lather do the work
  • Don't scrub lengths (unless very oily)—let lather rinse through
  • Rinse thoroughly with warm water, then finish with cool water to close cuticles
  • Follow with conditioner on mid-lengths to ends (yes, you still need this)
  • Optional acidic rinse: 1 tbsp apple cider vinegar in 1 cup water (see FAQ)
Natural shampoo bars drying on bamboo soap dish with drainage ridges
Finished bars


Storage

  • Let the bar dry completely between uses on a draining soap dish
  • Keep away from the direct shower spray
  • Cure for 48 hours before first use for a harder, longer-lasting bar
  • Shelf life: 6–12 months if kept dry (preservative protects against mold in humid environments)

Troubleshooting Table

Symptom

Likely Cause

Fix

Waxy, sticky buildup

Hard water + alkaline residue (if using soap-based)

Switch to the syndet recipe OR use an acidic rinse after every wash

Hair feels stripped/dry

Too much clay or not enough conditioning agents

Reduce clay to 1/2 tsp; increase BTMS or add 5g more oil

Bar crumbles or falls apart

Not enough liquid or not packed firmly in the mold

Add 5–10g more infusion/water; press VERY firmly when molding

Scalp itches after use

Allergic reaction or too much essential oil

Remove all EOs; switch to Recipe #2; test ingredients individually

No lather

SCI not fully melted OR very hard water

Melt SCI completely; add cocamidopropyl betaine for lather boost

Bar melts in the shower

High humidity + not cured long enough

Cure for 72 hours; store in a dry spot between uses

Hair tangles badly

Not enough conditioner OR skipped cool rinse

Increase BTMS to 30g; always use a separate conditioner; rinse with cool water


Common Mistakes (And How to Avoid Them)

Mistake #1: Not weighing ingredients.
Eyeballing doesn't work. Use a scale. 5g off can ruin your texture.

Mistake #2: Adding water without a preservative.
Water + no preservative = mold city in 2 weeks. Always use Leucidal SF or similar if your recipe includes infusions.

Mistake #3: Expecting instant perfection.
Your hair needs time to adjust. Give it 3–4 washes before deciding the bar doesn't work.

Mistake #4: Using soap-based bars in hard water without an acidic rinse.
If you have hard water and use a traditional soap bar, you WILL get buildup. Use a vinegar or citric acid rinse every time.

Mistake #5: Overloading with essential oils.
More is not better. Stick to 1–2% of total batch weight. Skin irritation isn't worth the extra scent.

Safety + Storage

Safety Notes

  • Preservative is non-negotiable if using any water-based ingredient (infusions, aloe, etc.)
  • Patch test any new bar on your inner arm for 24 hours before using it on your scalp
  • Keep bars away from children and pets (they look and smell nice, but aren't food)
  • If you experience persistent scalp irritation, stop use and consult a dermatologist.

Storage Best Practices

  • Cure bars in a cool, dry place with good airflow
  • Once cured, store extras in a breathable container (paper bag, not plastic)
  • Use a draining soap dish with ridges—sitting water = mushy bar
  • In very humid climates, store unused bars in an airtight container with silica gel packets
Disclaimer: These recipes are for personal use and educational purposes only. This blog does not provide medical advice. If you have scalp conditions, allergies, or medical concerns, consult a healthcare professional before trying new hair products. Results vary by individual hair type and water quality.

Frequently Asked Questions

Do I need a vinegar rinse?

For syndet bars (Recipes #1 and #2): No, not usually. These are pH-balanced and shouldn't leave alkaline residue.

For soap-based bars: Yes, especially if you have hard water. Mix 1 tablespoon apple cider vinegar in 1 cup of water and pour over hair after shampooing. This neutralizes alkaline residue and closes the cuticle.

Bottom line: Try your bar without the rinse first. If hair feels tangled or waxy, add an acidic rinse.

How long does a shampoo bar last?

One bar typically lasts 2–3 months with regular use, depending on hair length and frequency. They last much longer than you'd expect because you're not using a product with 80% water filler.

Can I use these on color-treated hair?

Yes. The syndet recipes are gentle enough for color-treated hair. Add hibiscus for reds/browns or chamomile for blondes to enhance color. Protein add-ins help strengthen chemically-treated hair.

Why is my bar melting in the shower?

Either it didn't cure long enough (needs 48–72 hours) or it's sitting in water. Use a draining soap dish and keep the bar out of direct shower spray. High-humidity climates need extra cure time.

Can I make these without SCI?

SCI is the backbone of these syndet recipes. Without it, you'd need to switch to a completely different formula (like a soap-based bar made with lye). SCI is available online from DIY cosmetic suppliers and is worth ordering for the best results.

Is this safe for kids?

Recipe #2 (Sensitive Scalp) is gentle enough for children over age 3, especially without essential oils. Always supervise use and avoid eye contact. For babies and toddlers, stick to pediatrician-recommended products.

My hair feels different—is that normal?

Yes. Transition from conventional shampoo takes 2–4 washes. Your scalp is adjusting to synthetic silicones and sulfates. Some people experience temporary oiliness or dryness before hair balances. Stick with it.

Can I add fresh herbs instead of dried?

No. Fresh herbs contain moisture that can introduce bacteria and shorten shelf life dramatically, even with a preservative. Always use dried herbs for infusions.

Do these work in hard water?

Syndet bars work MUCH better in hard water than soap-based bars. If you have extremely hard water and still experience issues, try a chelating shampoo once a month or install a shower filter.

Can I sell these bars?

If you want to sell DIY cosmetics, you need to follow FDA regulations, use proper good manufacturing practices (GMP), have proper insurance, and follow labeling laws. These recipes are shared for personal use only.

What if I'm allergic to coconut-derived ingredients?

SCI, BTMS, and cocamidopropyl betaine are all coconut-derived. If you have a true coconut allergy (rare but serious), consult an allergist before using. Some people react to whole coconut but tolerate highly-processed derivatives—test carefully.

How do I know if my bar has gone bad?

Signs of spoilage: off smell (rancid or musty), mold spots, color changes, or slimy texture. If properly preserved and stored dry, bars last 6–12 months. When in doubt, toss it.

Final Thoughts: Make It Yours

You now have everything you need to make a shampoo bar that actually works for your hair.

Start with Recipe #1 or #2 as written. Use it for a week. Then adjust.

Add rosemary if you want stimulation. Add clay if you're oily. Add extra conditioning if you're dry. This is your formula to customize.

Ready to Get Started?

Save this post so you can come back when you're ready to tweak your recipe. And drop a comment below with your hair type—I'd love to know which version you're planning to try first.

Want to print this recipe for your bathroom? Copy the ingredient tables into a document and laminate them. No more scrolling on a wet phone.

Now go make something that works.

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